Test Items | Standards | |
Appearance | Clear, colourless to slightly yellow or greenish-yellow, | |
| viscous, oily liquid | |
Solubility | Practically insoluble in water, freely soluble in acetone, in | |
| ethanol and vegetable oils | |
Assay | ≥98.0% | 99.2% |
Identification A, B, C | Correspond | confirm |
Related substances | Impurity A :≤0.5% | 0.07% |
| Impurity B :≤1.5% | 0.73% |
| Impurity C(free tocopherol) :≤0.5% | 0.2% |
| Sum of impurity D and E :≤1.0% | 0.15% |
| Any other impurity, for each impurity: ≤0.25% | 0.25% |
| Total: ≤2.5% | 1.6% |
Optical rotation | −0.01° to + 0.01° | confirm |
Acid Value | ≤2.0mg KOH/g | 0.09mg KOH/g |
Free tocopherol | ≤0.5% | 0.3% |
Sulphated ash | ≤0.10% | < 0.1%< 10 |
Heavy Metals | ≤10mg/kg | 10mg/kg |
Lead | ≤2mg/kg | 2mg.kg |
Arsenic | ≤1mg/kg | 1mg/kg |
Refactive index(20℃) | 1.494~1.498 | < 1mg/kg |
Absorbance | 42.0~45.0 Max. at about 284nm | confirm |
| 7.5~9.0 Min. at about 254nm | confirm |
Density(20℃) | 0.952~0.966g/ml | confirm |
Residual solvents | Meet the requirement | confirm |